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The in-lab preparation of certain chemical reagents provides a number of advantages over purchasing various commercially prepared samples. This is especially true in isolated regions where acquiring the necessary substances from overseas can cause undue delay and inconvenience due to restrictions on the transportation of hazardous chemicals. An invaluable resource for chemists in a variety of environments, Small-Scale Synthesis of Laboratory Reagents with Reaction Modeling presents efficient, sensible, and versatile methods for the laboratory preparation of common chemical reagents.Rapid, reliable synthesisDesigned to facilitate smooth experimentation in the lab, this volume presents preparations chosen for their short duration, availability of apparatus, high yield, and high purity of the product. Adding an educational component, the book also discusses fundamental processes in inorganic chemistry, presenting original modeling of reactions and their practical implementation. Theoretical aspects are discussed to a greater extent than is usual in synthetic literature in cases where there is a direct impact on experimental parameters, such as the reaction time, yield, and purity of the product.More than 30 convenient, time-saving preparationsFocusing on simple synthesis of high-purity reagents, the book contains over 30 presentations, a substantial number of which are mathematically modeled for the first time. Most syntheses can be carried out in one day using common laboratory equipment, making this volume a valuable and time-saving tool.
I’m and old chemist, and love the old chemistry books when researchers had to make reagents and not just order them. This has the flavor of those old texts with the big bonus of a detailed modeling of the reaction. A great blend of the old with the new. I really enjoyed this book and found it very informative. I would never try to make these highly reactive reagent, but understanding their chemistry though modeling was a big plus. Highly recommended.